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CINRG Particle-Counting Method for Fire-Resistant Water/Glycol Fluids

Why traditional optical particle counters fail on water/glycol hydraulic fluids — and the dilution method we developed to make D7647-style counting reliable on these samples.

Particle counting in water/glycol fluids

The importance of cleanliness in water/glycol hydraulic fluids and the challenges with particle counting. Hydraulic systems rely heavily on fluid cleanliness to ensure efficiency, longevity, and reliability. Among the various hydraulic fluids used in industrial applications, water/glycol-based fluids stand out for their unique properties — particularly their excellent fire resistance and ability to operate in harsh environments. However, maintaining cleanliness poses distinct challenges, especially when it comes to particle counting, a critical aspect of monitoring fluid health.

Why cleanliness matters in water/glycol fluids

Water/glycol hydraulic fluids are commonly used in industries such as steelmaking, mining, and aviation, where fire safety and thermal stability are paramount. Cleanliness of these fluids is crucial: contaminants like dirt, wear particles, and corrosion products can damage hydraulic components — causing premature wear of pumps, valves, and seals. Particulates can also influence the chemical stability of water/glycol fluids, potentially compromising their fire-resistant properties.

Given the criticality of cleanliness, regular monitoring of water/glycol fluids is essential. However, these fluids present unique challenges that make traditional particle-counting methods less effective.

Challenges in particle counting for water/glycol fluids

Particle counting is one of the most effective ways to assess hydraulic-fluid cleanliness. However, water/glycol fluids complicate this process due to their composition and behavior. Water/glycol fluids typically contain 35–50% water, which affects the optical properties of the fluid. Optical particle counters can misidentify water droplets as solid particles, leading to inflated particle counts and inaccurate cleanliness assessments.

To overcome these challenges, specialized methods and instruments are needed. The standard ASTM D7647-21 specifically addresses optical particle counting of hydraulic fluids containing water. By masking the influence of water droplets and soft particles, it provides a more reliable particle count. Automated particle counters like the CINRG CS-APC-3 and CS-APC-22M are designed to handle fluids with high water content and ensure accurate counts by masking the water present in the sample.

Particle-counting method for water/glycol fluids

CINRG has developed a straightforward method for accurate particle counting of water/glycol-based fire-resistant hydraulic fluids. This method substitutes the standard isopropanol/toluene solvent for EGBE, which has better water-masking properties.

Sample type
Water/Glycol-based Fire-Resistant Fluids (e.g., Houghton Houghto-Safe 620) typically have between 35% and 45% water.
Materials
Dilution solvent: Ethylene glycol butyl ether (2-Butoxyethanol) or DPnP (let settle for 12 hours).
Procedure
  1. Set stir speed to 6, using a minimum mixing time of 1 minute.
  2. Add 5 ml of sample to sample cup [sample:solvent] [1:5].
  3. Run samples using standard processing.
  4. If sample fails, reprocess adding only 1 ml of sample to sample cup [sample:solvent] [1:29].

Water/glycol hydraulic fluids are indispensable in many industries, but their unique composition requires extra attention to cleanliness and fluid monitoring. Accurate particle counting is a cornerstone of fluid-health management, but traditional methods often fall short when dealing with these complex fluids.

By adopting standards like ASTM D7647 and using advanced particle counters tailored to water/glycol fluids, industries can ensure accurate cleanliness assessments. This not only extends equipment life but also enhances operational reliability and safety, particularly in high-stakes environments where fire resistance and performance are non-negotiable. As hydraulic systems evolve, so too must our approaches to maintaining their vital fluids.

Posted by Bill Quesnel · June 5, 2023
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